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Torsional rigidity methods take advantage of the change in rigidity that occurs when a polymer passes through the glass transition temperature. One approach involves measuring the resistance to torsion and the energy loss of a bar of a polymer as the temperature is varied. A laboratory variation involves a torsional pendulum with a polymer sample impregnating a braided glass ber. A diagram of such a torsional pendulum is shown in Figure 3.27. A solution of the polymer is administered and dried. The impregnated ber is suspended in a constant-temperature medium, and the sample is heated. As it passes through the glass transition temperature, a large loss in rigidity occurs that can be detected by a change in the pendulum damping. It is a very sensitive method that only requires about a fourth of a gram of polymer. Broadline NMR is another method for noting glass transition temperatures. Below the glass transition temperature the solid exhibits broad, diffuse peaks, if any can be observed at all. When the polymer passes through the glass transition temperature, the polymer becomes more like a liquid and a narrow peak or series of narrow peaks occurs. The peak width can drop by an order of magnitude over a temperature range of just a few degrees. Dilatometry is a measurement of volume expansion versus temperature. A change in the slope of the line occurs at the glass transition temperature (and at the melting point for a crystalline polymer) as shown schematically in Figure 3.28. create barcode in excel 2013 free Using the Barcode Font in Microsoft Excel (Spreadsheet)
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